A compact and mobile stray-field NMR sensor #Instrumentation

Published: Monday, 20 January 2025 - 10:00 -0400

Author: Thorsten Maly

Alnajjar, Belal M.K., Jürgen Frick, Bernhard Blümich, and Jens Anders. “A Compact and Mobile Stray-Field NMR Sensor.” Journal of Magnetic Resonance 369 (December 2024): 107798.

https://doi.org/10.1016/j.jmr.2024.107798.

In this paper, we introduce a compact, single-sided stray field sensor for NMR relaxometry applications. The sensor consists of four main components: the magnet, the RF coil, the spectrometer, and the translation stage. Our proposed magnet, an improved design of the Profile NMR−MOUSE, is designed for low weight, compactness, and magnetic field homogeneity, achieved through various shim strategies using a mixed genetic algorithm. The magnet comprises eight NdFeB blocks, generating a magnetic field of 0.424 T within the sensitive region, positioned 12 mm above the magnet surface. For high spatial resolution measurements, we optimized the sensor performance by using a custom-designed rf coil, providing maximum sensitivity, lateral selectivity, and a dead time of less than 20 μs. Moreover, we utilized 3D-printed structures to precisely align the sensitive slice within the object, using an experimental approach based on CPMG measurements. The presented setup achieved a spatial resolution of 50 μm, with resolution changes proportional to acquisition time. We demonstrate the sensor’s versatility and high resolution with measurements on materials such as cosmetics, elastomers, glue, and wood, verifying the good performance of our design, our alignment strategy, and the measuring scheme.